|CXIDB ID 171|
|Title:||Structural insights into the mechanism of rhodopsin phosphodiesterase|
|Authors:||Tatsuya Ikuta et al.|
|Method:||Synchrotron Crystallography (small-wedge)|
|Wavelength:||1.00 Å (12.4 keV)|
|Raw Data:||180608_BL32XU/ (4 KB)|
|Raw Data:||180803_BL32XU/ (4 KB)|
Crystal structures of TMD of Rhodopsin phosphodiesterase (PDB code: 7CJ3). 6160 small-wedge (10°/crystal) datasets collected from loop-harvested microcrystals using EIGER X 9M detector at a wavelength of 1 Å on BL32XU, SPring-8. Beam size was around 15×10 µm2 and oscillation step was 0.1°. The crystals belonged to space group P212121 with unit cell parameters a~66, b~74, c~117 Å. 864 datasets were indexed and integrated using XDS with KAMO pipeline. Finally 271 integrated results were merged at 2.6 Å resolution after CC-based clustering and outlier rejection by KAMO in the published result.